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High Temperature X-Ray Diffraction in Transmission Under Controlled Environment

Published online by Cambridge University Press:  10 February 2011

L. Margulies,
M. J. Kramer,
J. J. Williams,
E. M. Deters,
R. W. McCallum,
D. R. Haeffner,
J. C. Lang,
S. Kycia and
A. I. Goldman
L. Margulies
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011, hanuman@iastate.edu
M. J. Kramer
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
J. J. Williams
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
E. M. Deters
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
R. W. McCallum
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
D. R. Haeffner
Affiliation:
APS, Argonne National Laboratory, Argonne, II 60439
J. C. Lang
Affiliation:
APS, Argonne National Laboratory, Argonne, II 60439
S. Kycia
Affiliation:
CHESS, Cornell University, Ithaca, NY 14853
A. I. Goldman
Affiliation:
Ames Laboratory, Iowa State University, Ames, IA 50011
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Abstract

A compact tube furnace has been developed for high temperature X-ray diffraction studies using high energy synchrotron radiation. The furnace design has a low absorption path in transmission yet allows for a high degree of control of the sample atmosphere and a minimal temperature gradient across the sample. The design allows for a maximum temperature of 1500°C with a variety of atmospheres including inert, reducing, and oxidizing. Preliminary results obtained at the SRI-CAT I-ID undulator line (60keV) at the APS facility and the A2 24 pole wiggler line (45keV) at CHESS on the Ti5Si3Z5 (Z = C, N, O) system will be presented to demonstrate the feasibility of this approach.

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References

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