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Characterization of Ceramic Batch Via Capillary Rheometry

Published online by Cambridge University Press:  15 February 2011

Victor F. Janas
Affiliation:
Corning Incorporated, Applied Process Research, EJ-114, Corning, NY 14831
Christopher J. Malarkey
Affiliation:
Corning Incorporated, Applied Process Research, EJ-114, Corning, NY 14831
David R. Treacy
Affiliation:
Corning Incorporated, Applied Process Research, EJ-114, Corning, NY 14831
Michael E. Zak
Affiliation:
Corning Incorporated, Applied Process Research, EJ-114, Corning, NY 14831
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Abstract

Rheological testing has been developed to predict the extrudability of ceramic pastes. Inorganic batches containing cellulosic binders were mixed in a twin screw extruder prior to characterization in a capillary rheometer. Various die lengths were used to separate viscosity from wall slip parameters. A power law model was fit to the paste viscosity. The wall shear stress, assuming 100% slip, was a linear function of the wall velocity. The resulting rheological models were used in fluid flow finite element analysis for determination of extrusion pressure, and the evaluation of binders.

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