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High-throughput preparation of multinary liquid, thin-film and powder library by combinatorial electrostatic atomization system

Published online by Cambridge University Press:  26 February 2011

Kenjiro Fujimoto,
Shigeru Ito,
Satoru Inoue and
Mamoru Watanabe
Kenjiro Fujimoto
Affiliation:
fujimoto@rs.noda.tus.ac.jp, Tokyo University of Science, Department of Pure and Applied Chemistry, Yamazaki 2641, Noda, Chiba, 278-8510, Japan, +81-4-7124-1501 X.3648, +81-4-7123-9890
Shigeru Ito
Affiliation:
ito@rs.noda.tus.ac.jp, Tokyo University of Science, Department of Pure and Applied Chamistry, Japan
Satoru Inoue
Affiliation:
inoue.satoru@nims.go.jp, National Institute for Materials Science, Japan
Mamoru Watanabe
Affiliation:
watanabe.mamoru@nims.go.jp, National Institute for Materials Science, Japan
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Abstract

A newly developed high-throughput exploration system “M-ist Combi” can control mixing ration of five-component compounds. Furthermore, the M-ist Combi system can also be obtained not only thin film but also powder and liquid libraries by controlling applied voltage and used flexibly in either a normal atmosphere or controlled atmosphere. By combining the M-ist Combi system with combinatorial XRD apparatus, we successfully completed the high-throughput powder preparation and phase identification of over 150 samples in one day.

Keywords

combinatorial synthesisx-ray diffraction (XRD)powder processing

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