Microelectromechanical Systems (MEMS) are being extensively investigated as a means of miniaturizing piezoelectric sensors thereby offering higher sensitivity, reduced power consumption, and ability to form compact multi-sensor arrays. Such devices typically employ one or more silicon micromechanical elements (e.g. membranes, cantilever beams and tethered proof masses) driven electromechanically by a polycrystalline piezoelectric film. The use of polycrystalline materials results in inherently less stable and irreproducible device characteristics. For elevated operating temperatures, more robust and refractory materials are also required. In this paper, we describe a MEMS microresonator array capable of operating to temperatures exceeding 600°C enabled by the integration of epitaxially grown piezoelectric AlN films onto single crystal SiC tethered plates. The operation of the microresonators as sensors is illustrated by examining their response to temperature, pressure and chemical analytes.