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New X-ray powder diffraction data for lithium tetrahydroxoborate LiB(OH)4

Published online by Cambridge University Press:  10 January 2013

M. Touboul
Affiliation:
Université de Picardie Jules Verne, Laboratoire de Réactivité et de Chimie des Solides, URA CNRS 1211, 33 rue Saint-Leu, 80039 Amiens cedex, France
E. Bétourné
Affiliation:
Université de Picardie Jules Verne, Laboratoire de Réactivité et de Chimie des Solides, URA CNRS 1211, 33 rue Saint-Leu, 80039 Amiens cedex, France
B. Gérand
Affiliation:
Université de Picardie Jules Verne, Laboratoire de Réactivité et de Chimie des Solides, URA CNRS 1211, 33 rue Saint-Leu, 80039 Amiens cedex, France
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Abstract

The X-ray powder diffraction pattern of hydrated lithium monoborate LiB(OH)4, sometimes formulated LiBO2·2H2O, has been obtained. Refinements of indexed reflections yielded the following parameters: a = 9.1732(7)Å, b = 7.9622(6)Å, c = 8.5354(8)Å, space group Pbca, Z = 8, Dx = 1.827, Dm = 1.83 g/cm3. The Smith–Snyder figure-of-merit is F30 = 101(0.007,44).

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Type
Research Article
Copyright
Copyright © Cambridge University Press 1994

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