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Published online by Cambridge University Press: 10 January 2013
Complete X-ray powder data is recorded from type specimens of the minerals nissonite and waylandite. Debye-Scherrer films of 114.59 mm diameter were measured with an automated densitometer. A wide step width of 0.08°2θ was required, because the average reflection width at half height was 0.5°2θ. The 2θ positions and relative intensities of the reflections were calculated from a negative second derivative function based upon a five point curve.