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X-ray powder diffraction analysis of a nonlinear optical material o–chlorobenzol–benzoyl thiourea

Published online by Cambridge University Press:  10 January 2013

Zong-ming Jin,
Bo Zhao,
Weiqun Zhou and
Zheng Jin
Zong-ming Jin
Affiliation:
Central Laboratory, Suzhou University, 1 Shizi Street, Suzhou, 215006, People's Republic of China
Bo Zhao
Affiliation:
Department of Chemistry, Suzhou University, 1 Shizi Street, Suzhou, 215006, People's Republic of China
Weiqun Zhou
Affiliation:
Biotechnics college, Suzhou University, 1 Shizi Street, Suzhou, 215006, People's Republic of China
Zheng Jin
Affiliation:
Suzhou Testing Institute of Technology, 5 Minzhi Road, Suzhou, 215006, People's Republic of China
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Abstract

A nonlinear optical material, o–chlorobenzol–benzoyl thiourea (C14H11ClN2OS), has been characterized by X-ray powder diffraction. Experimental values of 2θ corrected for systematic errors, relative peak intensities, values of d, and the Miller indices of 78 observed reflection with 2θ up to 72° are reported. The powder diffraction data have been evaluated, and the figures-of-merit are reported. The unit cell parameters least-squares refined from 28 nonoverlapping peaks of the monoclinic compound with a P2 space group are a=13.2797(4) Å, b=12.4058(8) Å, c=8.1561(2) Å, β=95.398(1)°, V=1337.7(4) Å3, Z=4, Dx=1.444 g/cm3. © 1997 International Centre for Diffraction Data.

Information

Type
Research Article
Information
Powder Diffraction , Volume 12 , Issue 1 , March 1997, pp. 47 - 48
Copyright
Copyright © Cambridge University Press 1997

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References

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