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X-ray powder diffraction analysis of a silver(I) cyclamate complex

Published online by Cambridge University Press:  01 March 2012

R. Putvinskis ,
C. O. Paiva Santos ,
M. Cavicchioli  and
A. C. Massabni
R. Putvinskis
Affiliation:
Laboratório Computacional de Análises Cristalográficas e Cristalinas - LabCACC, Instituto de Química, UNESP, 14800-900, Rua Prof. Francisco Degni s/n, Araraquara, SP, Brazil
C. O. Paiva Santos
Affiliation:
Laboratório Computacional de Análises Cristalográficas e Cristalinas - LabCACC, Instituto de Química, UNESP, 14800-900, Rua Prof. Francisco Degni s/n, Araraquara, SP, Brazil
M. Cavicchioli
Affiliation:
Departamento de Química Geral e Inorgânica, Instituto de Química, UNESP, 14800-900, Rua Prof. Francisco Degni s/n, Araraquara, SP, Brazil
A. C. Massabni
Affiliation:
Departamento de Química Geral e Inorgânica, Instituto de Química, UNESP, 14800-900, Rua Prof. Francisco Degni s/n, Araraquara, SP, Brazil
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Abstract

X-ray powder diffraction data collected for the complex silver(I) cyclamate [Ag(C6H12NO3S)] are reported. This material was obtained from a stoichiometric mixture of sodium cyclamate and AgNO3. The analysis of the data using the Le Bail method showed that the complex has monoclinic symmetry (space group C2/c). The unit cell parameters are a=31.85852(16) Å, b=6.25257(6) Å, c=8.46165(7) Å, and β=95.7651(5)°.

Keywords

silver(I)cyclamateX-ray powder diffractionLe Bail method

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Type
New Diffraction Data
Information
Powder Diffraction , Volume 22 , Issue 1 , March 2007 , pp. 68 - 70
Copyright
Copyright © Cambridge University Press 2007

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