Hostname: page-component-74656f9884-npj9w Total loading time: 0 Render date: 2026-11-10T21:36:32.465Z Has data issue: false hasContentIssue false
  • English
  • Français

X-ray powder diffraction data for ammonium hydrogen (acid) urate, NH4C5H3N4O3

Published online by Cambridge University Press:  10 January 2013

Rodney T. Tettenhorst  and
Roger E. Gerkin
Rodney T. Tettenhorst
Affiliation:
Department of Geological Sciences, Ohio State University, Columbus, Ohio 43210
Roger E. Gerkin
Affiliation:
Department of Chemistry, Ohio State University, Columbus, Ohio 43210
Get access

Abstract

Crystal and X-ray powder diffraction data are presented for the title compound. The powder pattern was indexed and refined on a monoclinic cell with a=17.356(6) Å, b=3.528(1) Å, c=11.285(1) Å, β=94.23(2) Å. The cell volume and Dm=1.772 g/cm3 give Z=4. The space group could not be determined with certainty. The planes of the urate anions likely are stacked parallel or nearly parallel to (010).

Information

Type
Research Article
Information
Powder Diffraction , Volume 14 , Issue 4 , December 1999 , pp. 305 - 307
Copyright
Copyright © Cambridge University Press 1999

Access options

Get access to the full version of this content by using one of the access options below. (Log in options will check for institutional or personal access. Content may require purchase if you do not have access.)

Article purchase

Temporarily unavailable

References

Boultif, A., and Louer, D. (1991). “Indexing of powder diffraction patterns for low symmetry lattices by the successive dichotomy method,” J. Appl. Crystallogr. 24, 987–993.CrossRefGoogle Scholar
Bovee, K. C., and McGuire, T. (1984). “Qualitative and quantitative analysis of uroliths in dogs: Determination of chemical type,” J. Amer. Vet. Med. Assoc. 185, 983–987.Google ScholarPubMed
Briggs, O. M., Rodgers, A. L., and Harley, E. H. (1982). “Uric acid urolithiasis in a Dalmatian coach hound,” J. So. Afr. Vet. Assoc. 53, 205–208.Google Scholar
Dubler, E., Jameson, G. B., and Kopajtić, Z. (1986). “Uric acid salts of magnesium: Crystal and molecular structures and thermal analysis of two phases of Mg(C 5H 3N 4O 3)2·H 2O,”J. Inorg. Biochem. 26, 1–21.CrossRefGoogle Scholar
Lewis, L. D., Morris, M. L. Jr., and Hand, M. S. (1987). “Canine urolithiasis,” in Small Animal Clinical Nutrition III, Chapter 10 (Mark Morris Associates, Topeka, KS), pp. 1–34.Google Scholar
Mandel, N. S., and Mandel, G. S. (1976). “Monosodium urate monohydrate, the gout culprit,” J. Am. Chem. Soc. 98, 2319–2323.CrossRefGoogle ScholarPubMed
Osborne, C. A., Clinton, M. T., and Bamman, L. K. (1986). “Prevalence of canine uroliths,” Vet. Clin. No. Amer. Small Anim. Pract. 16, 27–44.CrossRefGoogle ScholarPubMed
Sorenson, J. L., and Ling, G. V. (1993). “Diagnosis, prevention, and treatment of urate urolithiasis in Dalmatians,” J. Amer. Vet. Med. Assoc. 203, 863–869.CrossRefGoogle ScholarPubMed