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X-ray powder diffraction data for chioroquine sulphate monohydrate, C18H26CIN3·H2SO4·H2O

Published online by Cambridge University Press:  10 January 2013

D. F. Rendle  and
P. M. Cain
D. F. Rendle
Affiliation:
The Metropolitan Police Forensic Science Laboratory, 109 Lambeth Road, London SE1 7LP, United Kindgom
P. M. Cain
Affiliation:
The Metropolitan Police Forensic Science Laboratory, 109 Lambeth Road, London SE1 7LP, United Kindgom
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Abstract

X-ray powder diffraction data for chioroquine sulphate monohydrate [7—chloro—4—(4—diethylamino—1—methylbutylamino)—quinoline sulphate monohydrate, C18H26C1N3· H2SO4 · H2O] have been determined. Crystals of chioroquine sulphate monohydrate are orthorhombic, space group P212121 with a=9.0134(7), b=11.7417(6), c= 19.850(1) Å, Z=4, and Dx= 1.378 g cm−3. The F30 index is 121 (0.0062, 40).

Keywords

chioroquine sulphatepowder datadrugs of abuseforensic analysis

Information

Type
Research Article
Information
Powder Diffraction , Volume 8 , Issue 4 , December 1993 , pp. 221 - 222
Copyright
Copyright © Cambridge University Press 1993

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References

Appleman, D. E., and Evans, H. T. Jr., (1973). “Job 9214: Indexing and least-squares refinement of powder diffraction data,” U.S. Geol. Surv., Comput. Contrib. 20 (Rep. PB2-16188, U.S. Dept. of Commerce, National Technical Information Service, 5285 Port Royal Road, Springfield, VA 22151).Google Scholar
Benoit, P. H. (1987). “Adaptation to microcomputer of the Appleman Evans program for indexing and least-squares refinement of powder diffraction data for unit cell dimensions,” Am. Mineral. 72, 1018–1019.Google Scholar
Reynolds, J. E. F. (Ed.) (1989). Martindale: The Extra Pharmacopoeia (The Pharmaceutical Press, London), 29th ed.Google Scholar
McMurdie, H. F., Morris, M. C., Evans, E. H., Paretzkin, B.Wong-Ng, W., and Hubbard, C. R. (1986). “Methods of producing standard X-ray diffraction powder patterns,” Powd. Diffr. 1, 40–43.CrossRefGoogle Scholar
O'Gorman, P., Patel, S., Notcutt, S., and Wicking, J. (1987). Lancet 1, 746.CrossRefGoogle Scholar
Smith, G. S., and Snyder, R. L. (1979). “FN: A criterion for rating powder diffraction patterns and evaluating the reliability of powder pattern indexing,” J. Appl. Crystallogr. 12, 60–65.CrossRefGoogle Scholar