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Liquid Scintillation Counter Characterization, Optimization and Benzene Purity Correction

Published online by Cambridge University Press:  18 July 2016

F. G. McCormac*
Affiliation:
The Queen's University of Belfast, School of Geosciences, Palaeoecology Centre Belfast BT7 1NN, Northern Ireland
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Abstract

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In liquid scintillation counting (LSC), small variations in benzene purity can cause 14C pulse-height spectra to move with respect to the counting window. Thus, one must carefully monitor the purity of each benzene sample and apply corrections for spectral shifts. I describe here the techniques used at Queen's University Belfast for deriving correction factors for observed small variations in benzene purity. I also describe the methods used at our laboratory to fine-tune our Quantulus LS counters for high-precision dating. The tuning of the instruments minimizes the effect of fluctuations in gain that may occur during the long counting periods required for high-precision dating. Any remaining influences on efficiency owing to gain changes are corrected for, along with the purity correction, by continuous monitoring of the spectrum produced by the external source.

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Copyright © The American Journal of Science