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Detection of N-Containing Herbicides on Thin-layer Chromatograms

Published online by Cambridge University Press:  12 June 2017

D. C. Whitenberg
D. C. Whitenberg*
Affiliation:
Crops Research Division, Agricultural Research Service, U. S. Department of Agriculture, Crop Science Department, N.C. State University at Raleigh, Raleigh, N.C.
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Abstract

Herbicides which contain primary or secondary amino groups may be detected on thin layers of silica gel G or silica gel H with 1% tert-butyl hypochlorite, followed with an aqueous solution of 1% KI and 1% soluble starch. Detection limits range from approximately 1 μg to less than 0.05 μg, depending upon the herbicide in question. The technique also appears to be effective for aromatic or aliphatic iodides.

Information

Type
Brief Papers
Information
Weeds , Volume 15 , Issue 2 , April 1967, pp. 182
Copyright
Copyright © 1967 Weed Science Society of America 

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References

Literature Cited

1. Fieser, L. F. and Fieser, Mary. 1956. Organic Chemistry. D. C. Heath and Co., Boston, 1112 p.Google Scholar
2. Mazur, H., Ellis, B. W., and Cammarata, P. S. 1962. A new reagent for the detection of peptides, nucleotides, and other N-H containing compounds on paper chromatograms. J. Biol. Chem. 237:1619–1621.CrossRefGoogle ScholarPubMed