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Model for instrumented indentation of brittle open-cell foam

Published online by Cambridge University Press:  23 July 2018

Robert F. Cook*
Affiliation:
Materials Measurement Science Division, National Institute of Standards and Technology, Gaithersburg, MD 20899, USA
*
Address all correspondence to Robert F. Cook at robert.cook@nist.gov

Abstract

A model is developed and implemented for load-controlled instrumented conical indentation of a brittle open-cell foam on a dense substrate. A survey of observations suggests that such indentations are typified by displacement excursions at small indentation loads, load-displacement variability, localized crushing, and a discrete to continuum transition at intermediate loads. The model includes all these effects as well as stiffening at large loads as the substrate is encountered. Direct quantitative comparison is made with measurements of a silica foam on a soda-lime glass substrate, strongly supporting the physical basis of the model.

Information

Type
Research Letters
Copyright
Copyright © Materials Research Society 2018 
Figure 0

Figure 1. (a) Scanning electron microscope image of a silica open-cell foam showing the cells in a hexagonally close-packed array, the struts forming the cells, and the windows between the cells. (b) Indentation load-displacement, P-h, response for the silica foam, showing intermittent displacement excursions on loading comparable in scale to the cell diameter.

Figure 1

Figure 2. (a) Triangle load-time spectra used in the indentation model. The peak load, Pmax, was varied from 100 mN to 1 mN. (b) Schematic cross-sectional diagram of conical indentation of a foam on substrate system. The foam cell dimensions and thickness and indenter included angle are similar to those observed and modeled.

Figure 2

Figure 3. Flow diagram of the algorithm used to model foam indentation. The load was varied as in Fig. 2 and displacement determined via a reversible elastic path (left) or an irreversible fracture path (right) according to a critical pressure condition.

Figure 3

Figure 4. (a) The oscillatory variation of pressure with indentation displacement as modeled for a foam: x and x′ are stable configurations separated by an unstable configuration y. (b) The load-displacement behavior for a foam conjugate to (a) showing the displacement excursions under load-controlled indentation.

Figure 4

Figure 5. Direct experiment-model comparison of load-displacement, P-h, traces: (a) to (e) experimental observations for an open-cell silica foam at various peak indentation loads; (f) to (j) results of the model developed here using a critical pressure criterion for displacement excursion and including substrate effects. The variation in experimental P-h responses is due to microstructural effects, included in the model by variations in critical pressure.